Synthesis and Structural Analysis of Trichloroacetamidoxime

LC Bretanha, RA Freitag, GM Siqueira, M Ritter…

Index: Bretanha, Lizandra C.; Freitag, Rogerio A.; Siqueira, Geonir M.; Ritter, Marina; Campos, Patrick T.; Martins, Marcos A. P. Journal of Chemical Crystallography, 2012 , vol. 42, # 7 p. 697 - 700

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Abstract

Abstract The trichloroacetoamidoxime was synthesized following the principles of green chemistry in excellent yield (90%). This compound crystallizes in the orthorhombic system with space group P 2 1 2 1 2 1 and the cell parameters are a= 5.7353 (3), b= 10.5167 (8) Å, c= 21.4787 (16) Å, α, β and γ= 90°, V= 1295.52 (15) Å 3, Z= 4. The final residual factor is R 1= 0.0429, wR 2= 0.0884. The presence of the intermolecular hydrogen bonds generates ...