Facile synthesis and stabilization of 2-arachidonylglycerol via its 1, 3-phenylboronate ester
HH Seltzman, DN Fleming, GD Hawkins, FI Carroll
Index: Seltzman, Herbert H.; Fleming, Denise N.; Hawkins, Gregory D.; Carroll, F. Ivy Tetrahedron Letters, 2000 , vol. 41, # 19 p. 3589 - 3592
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Citation Number: 14
Abstract
2-Arachidonylglycerol (2-Ara-Gl) was synthesized via the intermediacy of its 1, 3- phenylboronic acid ester. The boronate ester is easily stable enough to enable chromatographic resolution from the corresponding 1-Ara-Gl boronate ester on normal phase elution yet immediately and completely hydrolyzes to 2-Ara-Gl and phenylboronic acid, without isomerization, by simple solution in aqueous-organic solvents. The ...
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