The Journal of Organic Chemistry

Synthesis and reactions of cyanovinyl substituted benzenediazonium salts for nonlinear optics

ML Schilling, HE Katz, DI Cox

Index: Schilling, M. L.; Katz, H. E.; Cox, D. I. Journal of Organic Chemistry, 1988 , vol. 53, # 23 p. 5538 - 5540

Full Text: HTML

Citation Number: 66

Abstract

Results Diazotization Reactions. The benzenediazonium salts are isolated by following the general procedure described by Roe8 for simple benzene derivatives. This involves diazotization of the aniline in HC1/H20 with sodium nitrite followed by precipitation of the fluoroborate salt by addition of sodium tetrafluoroborate (eq 1). Due to the low