Synthesis of 3??Deaza??2′??deoxyadenosine and 3??Deaza??2′, 3′??dideoxyadenosine: Glycosylation of the 4??Chloroimidazo [4, 5??c] pyridinyl Anion
F Seela, H Rosemeyer, S Fischer
Index: Helvetica Chimica Acta, , vol. 73, # 6 p. 1602 - 1611
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Citation Number: 17
Abstract
... The main amount of 7 crystallized from a small volume of AcOEt/cyclohexane 1: 1 upon cooling (5”). The filtrate was separated by FC (silica gel 60H, column 40 x 3 cm, 0.5 bar, AcOEt/cyclohexane 7:3), giving the less polar 8 (690 mg ... HELVETICA CHIMICA ACTA - Vol. 73 ( ...
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