Mild and useful method for N-acylation of amines
K Phukan, M Ganguly, N Devi
Index: Phukan, Kandarpa; Ganguly, Mausumi; Devi, Nirada Synthetic Communications, 2009 , vol. 39, # 15 p. 2694 - 2701
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Citation Number: 15
Abstract
Abstract Iodine is found to promote quantitative N-acylation of primary and secondary amines (aliphatic and aromatic) in a very short time with an equimolar amount of acetyl chloride and benzoyl chloride under solvent-free conditions at room temperature. This catalytic acylation of amines offers an additional useful method for the acetylation using acetyl chloride instead of acetic anhydride and other acetylating agents. This method is ...
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