Journal of the American Chemical Society

New Compounds. Alkyl Selenocyanates

W Weaver, W Whaley

Index: Weaver; Whaley Journal of the American Chemical Society, 1946 , vol. 68, p. 2115

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Citation Number: 5

Abstract

A variation in reaction conditions has produced this new compound instead of the 1, 3, 5-tri- p-toluenesulfonylcyclo-trimethylenetriamine reported by McMaster.'To 0.05 mole (7 9.) of hexamethylenetetramine in 80 cc. of water was added 0.199 mole (37.8 g.) of p- toluenesulfonyl chloride. To this stirred solution, covered with 60 cc. ether, was added 53 cc. of a 1570 aqueous sodium hydroxide solution (0.199 mole, 7.95 g. sodium hydroxide) at ...