The synthesis of [3H] and [14C] o??chlorobenzylidenemalononitrile (CS)
JM Harrison, TD Inch, IW Lawston…
Index: Harrison; Inch; Lawston; Ley; Sainsbury Journal of Labelled Compounds and Radiopharmaceuticals, 1978 , vol. 14, # 1 p. 141 - 148
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Abstract
Abstract Using similar procedures, the syntheses of [2-14 C]-malononitrile and malono [14 C] nitrile are described. Condensation with o-chlorobenzaldehyde affords [2-14 C]-o- chlorobenzylidenemalononitrile and o-chlorobenzylidenemalono [14 C] nitrile respectively. The syntheses of [3 H] o-chlorobenzaldehyde and o-chlorobenz [14 C] aldehyde, again by a common sequence of reactions, is described and with malononitrile gives [3 H]-o- ...
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