The Journal of Organic Chemistry

Synthesis of the N-isobutylamide of all-trans-2, 6, 8, 10-dodecatetraenoic acid

PE Sonnet

Index: Sonnet,P.E. Journal of Organic Chemistry, 1969 , vol. 34, p. 1147 - 1149

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Citation Number: 15

Abstract

Vol. $4, No. 4, April 1969 NOTES 1147 ether was added dropwise at room temperature to an equimolar mixture of an alkyl isocyanide and a Schiff base of benzaldehyde in 10 ml of ethyl ether. A white precipitate appeared immediately. The reaction system was kept at room temperature for 1 day. Then a water-methanol mixture was added to terminate the reaction. The precipitate was washed with petroleum ether, extracted with chloroform and finally ...