Development of a tandem base-catalyzed, triphenylphosphine-mediated disulfide reduction-Michael addition
A Bartolozzi, HM Foudoulakis, BM Cole
Index: Bartolozzi, Alessandra; Foudoulakis, Hope M.; Cole, Bridget M. Synthesis, 2008 , # 13 p. 2023 - 2032
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Citation Number: 9
Abstract
Abstract A tandem disulfide reduction-Michael addition was developed using both free and polymer-bound triphenylphosphine as the reducing agent. The procedure was applied to intermolecular systems for the synthesis of arylsulfanyl-and alkylsulfanyl-substituted propanoates and related ketones, and to an intramolecular system for the synthesis of a benzothiazepinone derivative.
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