Journal of the Iranian Chemical Society

Convenient synthesis of alkyl thioacetate from alkyl halide using a polymer-supported sodium thioacetate

MAK Zarchi, M Nejabat

Index: Zarchi, Mohammad Ali Karimi; Nejabat, Mojgan Journal of the Iranian Chemical Society, 2012 , vol. 9, # 5 p. 767 - 774

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Abstract

Abstract Alkyl halides are efficiently converted to their corresponding S-alkyl thioacetates under mild and nonaqueous conditions, using polymer-supported sodium thioacetate as a new polymeric reagent at room temperature in high yields and purity. The spent polymeric reagent can be removed quantitatively by filtration and pure products can be obtained by evaporation of the solvent. The spent polymeric reagent can be regenerated and reused ...