Hydrogen Transfer. II. Reaction of Diisopropyltoluene and Isopropylcyclohexyltoluene with Methylcyclohexene1

H Pines, A Weizmann, VN Ipatieff

Index: Pines; Weizmann; Ipatieff Journal of the American Chemical Society, 1948 , vol. 70, p. 3859,3861

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Citation Number: 21

Abstract

tion of 1 g. of 1'111 was reduced by the method PreviOuSlY described for VII. Evaporatio: of the ether left 0.68 g. of massive crystals, mp 99-101. Crystallization from dilute ethanol gave 0.45 g., mp 101-103". A mixture of this and the alcohol isolated from the ether preparatfi was fused, allowed to solidify and remelted at 103-105. The mother liquor from the ethan: l crystallization gave a second crop, 0.10 g., mp 101-102. This was converted into the ...