Journal of Chemical and Engineering Data

Preparation of sterically hindered phosphoramidates

JJ Talley

Index: Talley, John J. Journal of Chemical & Engineering Data, 1988 , vol. 33, # 2 p. 221 - 222

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Citation Number: 15

Abstract

Treatment of phosphorus oxychloride with two equivalents of 2, 64methyIphend In the presence of magnedum chloride produced the sterlcally hlndered bls (2, 8dhnethylphenyl) chlorophosphate In excellent yield. The dlaryl phosphorochlorldete reacted with a variety of primary and secondary amines to produce phosphoramldates In good to excellent yield.