The Preparation of Phosphonyl Chlorides by the Reaction of Hydrocarbons with Phosphorus Trichloride and Oxygen
WL Jensen, CR Noller
Index: Jensen; Noller Journal of the American Chemical Society, 1949 , vol. 71, p. 2384
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Citation Number: 19
Abstract
In the reaction of cyclohexane, it was noted that hydrolysis of the residue remaining after removal of unreacted reagents and phosphorus oxychloride gave only 60-75y0 of the amount of cyclohexanephosphonic acid expected from the weight of the residue, assuming it to be cyclohexanephosphonyl chloride. From the mother liquors a second material has been isolated which was difficult to obtain in solid form and which potentiometric titration curves ...
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