Journal of the American Chemical Society

The Isomerization of Dicyclohexy1

M Orchin, J Feldman

Index: Orchin; Feldman Journal of the American Chemical Society, 1946 , vol. 68, p. 2737

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Citation Number: 5

Abstract

Experimental (CH,), SiF,(CH,)? SiF,, CH3SiF3.-These compounds were prepared in a three- necked flask by adding the corresponding chlorosilane* to technical zinc fluoride that ha: been dried at 110'for twenty-four hours and cooled to 30 in the flask. The gas that was evolved in each case was passed through a water-cooled reflux condenser (which returned some of the unreacted chlorosilane), to a trap cooled by a mixture of Dry Ice and acetone. ...