Journal of the American Chemical Society

THE CHEMISTRY OF DIARYL SULFIDES. III. THE SYNTHESIS OF THIOTHYRONINE1

GH Law, TB Johnson

Index: Law; Johnson Journal of the American Chemical Society, 1930 , vol. 52, p. 3623,3625

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Citation Number: 4

Abstract

Experimental Part p-Ethoxythiophenol, CzH50C6HHSH.-'J! his thiophenol has previously been prepared by Lagaig and also Gattermann.'o By application of the technique of Leuckartll we succeeded in preparing the same compound in good yield (7770) from p- phenetidine. Ninety-six grams of the amine is productive of 83-85 g. of the thiophenol distilling between 238-241'. p-Ethoxy-p'-nitrodiphenyl-sulfide, C2H60C~ H4SCsH4N0*.- ...