Journal of the American Chemical Society

The Reaction of Diazoketones with Heterocyclic Amine Salts

LC King, FM Miller

Index: King; Miller Journal of the American Chemical Society, 1948 , vol. 70, p. 4154

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Citation Number: 4

Abstract

82 ") was subjec .e: to the Barbier-Wieland degradation cyclohexanecarboxylic acids and the cis- and trans- under previously described14 conditions except that the p- (2-pheny~cyc~ohexane ) -propionic acids have time of refluxing with acetic anhydride was increased to two and one-half hours. The crude product (IIIb) con; ... (previous softening). Recrystal1i:ation from hexane gave degradation, to the configurationally established colorless plates, mp 113.5-114.5 , ...