Organic letters

Palladium− Indolylphosphine-Catalyzed Hiyama Cross-Coupling of Aryl Mesylates

CM So, HW Lee, CP Lau, FY Kwong

Index: Organic Letters, , vol. 11, # 2 p. 317 - 320

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Citation Number: 74

Abstract

... Organic Letters. ... Among the commonly used organic solvents we examined, t-BuOH and toluene/t-BuOH mixtures gave the best results (entries 1−6). We next tested other ... 2:2; Pd(OAc) 2 /CM-phos = 1:4; 90 °C for 16 h in the specified solvent (1.0 mL, total solvent volume) under ...