Synthesis of Muramyl Peptides Containing meso??Diaminopimelic Acid
N Kubasch, RR Schmidt
Index: Kubasch, Niels; Schmidt, Richard R. European Journal of Organic Chemistry, 2002 , # 16 p. 2710 - 2726
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Citation Number: 17
Abstract
Abstract Chain-extension of L-glutamate aldehyde 3 by means of the Wittig− Horner reaction furnished the desired C 7 dicarboxylic acid derivative, which in turn, after CC double bond hydrogenation and protecting group manipulation, afforded the 2, 6-diaminopimelic acid derivatives (S, R)-9 and (S, S)-9, both with the desired orthogonal protecting group pattern. Synthesis of the muramic acid derivative 15 and attachment of an L-alanine residue ...
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