(Fluoroorgano) fluoroboranes and-fluoroborates I: synthesis and spectroscopic characterization of potassium fluoroaryltrifluoroborates and fluoroaryldifluoroboranes

HJ Frohn, H Franke, P Fritzen, VV Bardin

Index: Journal of Organometallic Chemistry, , vol. 598, # 1 p. 127 - 135

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Citation Number: 93

Abstract

... Journal of Organometallic Chemistry. ... 20.5 mmol) in ether (40 ml) was cooled to 0°C and added gradually to the solution of B(OCH 3 ) 3 (4.20 g, 40 mmol) in ether (20 ml) at 0°C. After stirring at 0°C for 1 h, the suspension was poured into 5% HCl (50 ml), the organic layer was ...