Tetrahedron

Oxaphospholene and oxaphosphinene heterocycles via RCM using unsymmetrical phosphonates or functional phosphinates

P Fourgeaud, C Midrier, JP Vors, JN Volle, JL Pirat…

Index: Tetrahedron, , vol. 66, # 3 p. 758 - 764

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Citation Number: 31

Abstract

... Tetrahedron. Volume 66, Issue 3, 16 January 2010, Pages 758–764. ... Cl), 2.25–2.15 (m, 2H, P-CH 2 ), 1.32 (t, 3 J HH =7.0 Hz, 6H, 2CH 3 ); 13 C NMR (62.90 MHz, CDCl 3 ): δ 61.5 (d, 2 J PC =6.5 Hz, OCH 2 ), 34.8 (s, CH 2 Cl), 29.9 (d, 1 J PC =140.0 Hz, P-CH 2 ), 15.3 (d, 3 J PC ...

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