Some γ-Substituted Benzoquinoline Derivatives1

RE Foster, RD Lipscomb, TJ Thompson…

Index: Foster et al. Journal of the American Chemical Society, 1946 , vol. 68, p. 1327,1330

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Citation Number: 8

Abstract

2-Chloro-4-methoxyquinazoline2 (3.0 g.) and 4.8 g. of purified! oval diamine'were heated two and a half hours at 125-130. The thick oil was dissolved in 40 cc. of 6 N hydrochloric acid and the solution heated six hours on the steam-bath. Then 20 cc. of concentrated hydrochloric acid was added and thesolution allowed to stand overnight. The solution was made strongly alkaline with sodium hydroxide, and was extracted with ether. Between the ...