Derivatives of Piperazine. VI. Alkylation by Means of Aldehydes
WT Forsee Jr, CB Pollard
Index: Forsee; Pollard Journal of the American Chemical Society, 1935 , vol. 57, p. 1788
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Citation Number: 6
Abstract
1788 WT FORSEE, JR., AND CB POLLARD ... Experimental Part4 The o-toluyl chloride used in this work was made from the acid by the use of thionyl chloride; yield, 89%; bp 212', corr. 3-o-Toluylacenaphthene (III).-Anhydrous aluminum chloride (30 g.) was added slowly, a little at a time, to an ice-cold mixture of 30 g. of pure acenaphthene and 30 g. of o-toluyl chloride in 75 cc. of carbon disulfide. After six hours at 0-5' the mixture was allowed to warm gradu- ...
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