Synthesis and spectral properties of diethyl organylchalcogenoalkyl (alkyl) malonates, RX (CH 2) n CR′(COOC 2 H 5) 2, and 5-alkyl-5-(organylchalcogenoalkyl) …
RA Grigsby, KJ Irgolic, FF Knapp
Index: Grigsby, Robert A.; Irgolic, Kurt J.; Knapp, Furn F. Journal of Organometallic Chemistry, 1983 , vol. 253, # 1 p. 31 - 38
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Abstract
Abstract Barbiturates substituted at the 5-position with organyltelluroalkyl or organylselenoalkyl groups were prepared by ring annulation of appropriately substituted diethyl malonates with urea or thiourea. The substituted diethyl malonates [phenyl- tellurobutyl (ethyl), i-propyltelluropropyl (ethyl), i-propyltelluropropyl (allyl), i- propylselenopropyl (ethyl), and phenylselenohexyl (methyl) were prepared in 55–91% ...
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