Synthesis and structure of substituted 5??phenoxy??1, 2, 4??dithiazole??3??ones

O Ponomarov, Z Padělková…

Index: Ponomarov, Oleksandr; Padelkova, Zdenka; Hanusek, Jiri Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 6 p. 1225 - 1228

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Abstract

Abstract Seven new substituted 5-phenoxy-1, 2, 4-dithiazole-3-ones were prepared in modest yield (53–76%) from corresponding O-phenyl thiocarbamates and chlorocarbonylsulfenyl chloride in dry ether at− 10 C. All of the compounds were characterized by NMR and elemental analysis and some of them by X-ray diffraction. Preliminary kinetic measurements showed that the parent 5-phenoxy-1, 2, 4-dithiazole-3- ...