Design and synthesis of bombykol analogues for probing pheromone-binding protein–ligand interactions
…, V Klusák, P Nešněrová, A Muck, J Doubský, A Svatoš
Index: Mansurova, Madina; Klusak, Vojtech; Nesnerova, Petra; Muck, Alexander; Doubsky, Jan; Svatos, Ales Tetrahedron, 2009 , vol. 65, # 5 p. 1069 - 1076
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Citation Number: 4
Abstract
Mono-, difluorinated, and thioanalogues of Bombyx mori female sex pheromones (bombykol, 1) were designed according to the ab initio calculations. These rationally designated analogues were synthesized using hydroboration and Sonogashira coupling strategy via (5E, 7Z)-undecadien-1-ol (10) as a common intermediate. A new simplified binding assay based on nanoLC-linear ion trap ESI-MS for quantifying complexation of ...
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