Pyrolysis of Esters. XXIII. 2, 3-Divinyl-1, 3-butadiene1-3
WJ Bailey, NA Nielsen
Index: Bailey,W.J.; Nielsen,N.A. Journal of Organic Chemistry, 1962 , vol. 27, p. 3088 - 3091
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Citation Number: 14
Abstract
C, 66.7; H, 4.71. 3-(a-Acetonylbenzyl)-4-methoxycoumarin (XV).-To a stirred benzene solution of 0.015 mole of dimethylcadmium8 was added 2.7 g.(0.015 mole) of XIV. The mixture was refluxed 15 min. and poured into 100 ml. of 5% hydrochloric acid and 50 ml. of ethyl acetate. The organic phase wag separated and washed with 100-ml. portions of water, 5% sodium hydroxide and water.-4fter drying with magnesium sulfate the solution was ...
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