Journal of the American Chemical Society

Hydroxyphenyl Alkyl Sulfides1

E Miller, RR Read

Index: Miller; Read Journal of the American Chemical Society, 1933 , vol. 55, p. 1224,1225

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Citation Number: 19

Abstract

I. p-Hydroxyphenyl Butyl Sulfide by the Thiohydroquinone Method.-Twenty grams of sodium hydroxide (0.5 mole) was partially dissolved in 50 g. of methyl alcohol and to this added a solution of 58.3 g. of thiohydroquinone (0.55 mole) in 50 g. of methyl alcohol. The mixture was stirred while 68 g. of n-butyl bromide (0.5 mole) was being added during the course of fifteen minutes. Reaction set in at once and proceeded vigorously with evolution of heat ...

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