Alkylation-reduction of carbonyl systems. VIII. Synthesis of. beta.,. gamma.-unsaturated aromatic hydrocarbons by tandem phenylation-reduction of. alpha.,. beta.- …
FJ McEnroe, CK Sha, SS Hall
Index: McEnroe,F.J. et al. Journal of Organic Chemistry, 1976 , vol. 41, p. 3465 - 3468
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Citation Number: 10
Abstract
Table I (Footnotes) a Small scale reaction using 2.5 mmol of carbonyl compound. See the Experimental Section for details. b In this and previous studies, the reactions were performed on a small scale and for mechanistic reasons with a large excess of lithium. Included in this work are the optimal conditions for a scaled-up synthesis (25 mmol) using the minimal amount of lithium. See Experimental Section for details. c Analyzed by GLC ( ...
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