Journal of medicinal chemistry

Sympathetic Nervous System Blocking Agents. III. Derivatives of Benzylguanidine1-3

JH Short, TD Darby

Index: Short,J.H.; Darby,T.D. Journal of Medicinal Chemistry, 1967 , vol. 10, p. 833 - 840

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Citation Number: 53

Abstract

Septenibcr 1967 SYMPATHETIC SERVOUS SYSTEM BLOCKING Lj2C; E; NTS. 111 833 yielded t, hree fractions (if bp (0.3 mm) 79-91, 134-142, and 14. il. iX". The second fraction was redist'illed [bp 132-136'(0.3 mni), 31 g] arid then crystallized from pentane at-40" ta afford pure 3-benzylindene as colorless prisms, mp 31.5-33"(lit. 3'mp 38-34'), yield 27.1 g (277,). The last fraction solidified in the condenser and was recrystallized fi, oin petroleum ...