Copper??Catalyzed Selective Oxidative Acylation of Secondary Anilines with Ethyl Glyoxalate: Domino Synthesis of Indoline??2, 3??diones
T Liu, H Yang, Y Jiang, H Fu
Index: Liu, Tao; Yang, Haijun; Jiang, Yuyang; Fu, Hua Advanced Synthesis and Catalysis, 2013 , vol. 355, # 6 p. 1169 - 1176
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Citation Number: 22
Abstract
Abstract A novel, easy and useful copper-catalyzed selective acylation of secondary anilines with ethyl glyoxalate has been developed, and the corresponding indoline-2, 3-dione derivatives were prepared. The procedure comprises the sequential intermolecular copper- catalyzed selective oxidative ortho-site aromatic acylation of the NH group in secondary anilines and intramolecular nucleophilic attack of the NH group to the ester. The ...
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