The Journal of Organic Chemistry
Compounds Containing the Trifluoromethyl Group1
EB Davidson, CG Overberger
Index: Davidson,E.B.; Overberger,C.G. Journal of Organic Chemistry, 1962 , vol. 27, p. 2267 - 2269
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Citation Number: 3
Abstract
Ethyl 3-Hydroxy-3-trifluoromethylbutyrate.-Half of a solution composed of trifluoroacetone 51 g.(0.46 mole), and dry benzene, 250 ml., was added to activated zinc powder, 32 g.(0.5@;.- atom). The materials were heated until reaction commenced, after which the remaining solution was added at a rate such that gentle refluxing was
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[McBee,E.T. et al. Journal of the American Chemical Society, 1962 , vol. 84, p. 3154 - 3157]