… , and spectroelectrochemistry of hypervalent Phosphorus (V) octaethylporphyrins and theoretical analysis of the nature of the PO bond in P (OEP)(CH2CH3)(O)

K Akiba, R Nadano, W Satoh, Y Yamamoto…

Index: Field, Steven J.; Young, Douglas W. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 591 - 594

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Citation Number: 35

Abstract

... Select a Journal or Book ... was stirred for 10 h, pure [P(OEP)(Cl) 2 ] + PF 6 - (1-PF 6 , 490 mg, 45%) was obtained by extraction with dichloromethane/water followed by recrystallization from dichloromethane/n-hexane (1:1). 1-PF 6 : 1 H NMR (CDCl 3 ) δ 1.87 (t, 24 H, J = 7.8 Hz ...