A rapid and efficient synthesis of symmetrical disulfides under microwave irradiation conditions
JX Wang, L Gao, D Huang
Index: Wang, Jin-Xian; Gao, Lijuan; Huang, Danfeng Synthetic Communications, 2002 , vol. 32, # 7 p. 963 - 969
Full Text: HTML
Citation Number: 28
Abstract
ABSTRACT A rapid and general method for the synthesis of symmetrical disulfides involves reaction of sulfur with sodium hydroxide under PTC-microwave irradiation condition to give sodium disulfide, which reacts with alkyl halides to afford the disulfides in good to excellent isolated yields.
Related Articles:
Easy and rapid method for disulfide syntheses using nanophase-manganese (VII) oxide coated clay
[Gondi, Sudershan R.; Son, David Y.; Biehl, Edward R.; Vempati, Rajan K. Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 1 p. 34 - 39]
[Bulletin of the Chemical Society of Japan, , vol. 56, # 9 p. 2657 - 2660]
A Facile Synthesis of Unsymmetrical Thiolsulfonates via Sulfonylation of Mercaptans1
[Ranasinghe, M. G.; Fuchs, P. L. Synthetic Communications, 1988 , vol. 18, # 3 p. 227 - 232]
S??Nitrosothiol and Disulfide Formation through Peroxynitrite??Promoted Oxidation of Thiols
[European Journal of Organic Chemistry, , # 1 p. 131 - 135]
[Scholz, Roland; Hellmann, Gunther; Rohs, Susanne; Oezdemir, Diana; Raabe, Gerhard; Vermeeren, Cornelia; Gais, Hans-Joachim European Journal of Organic Chemistry, 2010 , # 24 p. 4588 - 4616]