Cleavage of. alpha.,. alpha.'-dinitrocyclanones

H Feuer, AM Hall, RS Anderson

Index: Feuer,H. et al. Journal of Organic Chemistry, 1971 , vol. 36, # 1 p. 140 - 142

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Citation Number: 6

Abstract

O? NCBr,(CH2), CBr, h'OL tion was also successful with compound 5 as ascertained from infrared and nmr spectra of the crude reaction product. However, attempts to purify the crude ester by glpc or vacuum distillation led to decomposition. The structure of 9 and 10 was confirmed by spectral data and by conversion to the corresponding a, a, w, w-tetrabromo-a, w-dinitroalkanes on treatment with bromine in alkaline medium (eq 4). Compounds 9 and ...