Syntheses in the Quinoxaline Series. Preparation of 7-Methoxy-5-aminoquinoxaline and 7-Methoxy-5-hydroxylaminoquinoxaline

RH Mizzoni, PE Spoerri

Index: Mizzoni; Spoerri Journal of the American Chemical Society, 1945 , vol. 67, p. 1652

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Citation Number: 4

Abstract

solution of sodium methylate, prepared by dissolving 2.85 g. sodium (0.124 atom) in 30 cc. of absolute methyl alcohol, was placed in an ice-cooled three-necked flask, equipped with rdux condenser, mercury-sealed stirrer and dropping funnel, and a cooled solution of 5.95 g.(0.124 mole) of methyl mercaptan in 25 cc. of absolute methyl alcohol