Improvement of a critical intermediate step in the synthesis of a nitroxide-based spin-labeled deoxythymidine analog

JH Powell, EM Johnson, PM Gannett

Index: Molecules, , vol. 5, # 12 p. 1244 - 1250

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Citation Number: 14

Abstract

... to a pyrrolin-N-oxyl molecule [2]. The synthesis of this spin-labeled nucleic acid begins with stable nitroxides described by Rozantsev [3]; further elaboration of these ... Molecules 2000, 5 ... Method 5 – To a solution of 1 (1.84 g, 10 mmol) in dry THF (10 mL) was added, dropwise, a ...