A new, highly efficient method for the conversion of alcohols to thiolesters and thiols
RP Volante
Index: Volante, R. P. Tetrahedron Letters, 1981 , vol. 22, # 33 p. 3119 - 3122
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Citation Number: 221
Abstract
Abstract Various alcohols were converted to their corresponding thiolacetates by treatment with triphenylphosphine and diisopropyl azodicarboxylate in the presence of thiolacetic acid. The overall conversion was both highly efficient (89–99% yields) and stereoselective (99.5% inversion).
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