Palladium catalyzed reductive deprotection of Alloc: Transprotection and peptide bond formation
…, L Neuville, M Bois-Choussy, J Chastanet, J Zhu
Index: Beugelmans, Rene; Neuville, Luc; Bois-Choussy, Michele; Chastanet, Jacqueline; Zhu, Jieping Tetrahedron Letters, 1995 , vol. 36, # 18 p. 3129 - 3132
Full Text: HTML
Citation Number: 47
Abstract
N-allyloxycarbonyl group could be efficiently removed using sodium borohyride as hydride donnor in the presence of catalytic amount of palladium (0). The conditions were applied to chemoselective protecting group transformation (transprotection) and peptide bond formation.
Related Articles:
Synthesis of N-Methyl L-Phenylalanine for Total Synthesis of Pepticinnamin E
[Sun, Dequn; Zhang, Lingzi; Wang, Jin Asian Journal of Chemistry, 2012 , vol. 24, # 1 p. 319 - 322]
Synthesis of carbamates using yttria-zirconia based Lewis acid catalyst
[Pandey, Rajesh K.; Dagade, Sharda P.; Dongare, Mohan K.; Kumar, Pradeep Synthetic Communications, 2003 , vol. 33, # 23 p. 4019 - 4027]
[Hattori, Kazuyuki; Sajiki, Hironao; Hirota, Kosaku Tetrahedron, 2000 , vol. 56, # 43 p. 8433 - 8441]
[Sakaitani, Masahiro; Ohfune, Yasufumi Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 870 - 876]
[Barrett, Anthony G. M.; Pilipauskas, Daniel Journal of Organic Chemistry, 1990 , vol. 55, # 17 p. 5170 - 5173]