Bioinspired Synthesis of a Sedaxane Metabolite Using Catalytic Vanadyl Acetylacetonate and Molecular Oxygen

S Tyagi, CD Cook, DA DiDonato, JA Key…

Index: Concellon, Jose M.; Rodriguez-Solla, Humberto; Simal, Carmen Organic Letters, 2007 , vol. 9, # 14 p. 2685 - 2688

Full Text: HTML

Citation Number: 4

Abstract

... Volume: Page: ... The Journal of Organic Chemistry. ... during the workup using 10% H 2 SO 4 to form the amine 5. The standard deprotection conditions for the removal of the diphenylimine protecting group requires refluxing in aqueous mineral acid (6 M HCl) for a ...