Effective Methods for the Synthesis of N??Methyl β??Amino Acids from All Twenty Common α??Amino Acids Using 1, 3??Oxazolidin??5??ones and 1, 3??Oxazinan??6??ones
AB Hughes, BE Sleebs
Index: Helvetica Chimica Acta, , vol. 89, # 11 p. 2611 - 2637
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Citation Number: 18
Abstract
... Helvetica Chimica Acta – Vol. 89 (2006) 2622 ... The 1,3-oxazinan-6-one (1mmol) was dissolved in the minimum volume of CH2Cl2/ CF3CO2H 1:1 (v/v). Et3ACHTUNGTRENNUNGSiH (3 mmol) was added, and the mixture was stirred for 24–48 h, until no 1,3-oxazinan-6-one ...
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