Synthesis of 5??Aryl??3??Glycosylthio??4??Phenyl??4H??1, 2, 4??Triazoles and Their Acyclic Analogs Under Conventional and Microwave Conditions
…, ES Ramadan, SM Abdel??Maggeed…
Index: El-Ashry, El Sayed H.; Rashed, Nagwa; Awad, Laila F.; Ramadan, El Sayed; Abdel-Maggeed, Somia M.; Rezki, Nagat Journal of Carbohydrate Chemistry, 2008 , vol. 27, # 2 p. 70 - 85
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Citation Number: 13
Abstract
Under microwave irradiation (MWI), 4??phenyl??5??substituted??4H??1, 2, 4??triazole??3??thiol derivatives 7 and 8 were synthesized in a good yield by intramolecular cyclization of the aroyl phenyl thiosemicarbazides 5 and 6. The respective triazolylglycosides (Str??glycosides) 12–17 were obtained by reaction of triazoles 7 and 8 with glycosyl halides 9–11 in dry acetone in the presence of potassium carbonate as base under both conventional and ...
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