The Journal of organic chemistry

Synthesis of the proposed structure of mucoxin via regio-and stereoselective tetrahydrofuran ring-forming strategies

RS Narayan, B Borhan

Index: Fujioka, Hiromichi; Kitagawa, Hidetoshi; Kondo, Michinori; Matsunaga, Naoki; Kitagaki, Shinji; Kita, Yasuyuki Heterocycles, 1993 , vol. 35, # 2 p. 665 - 669

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Citation Number: 54

Abstract

... Volume: Page ... manner by LAH reduction, and the alcohol was protected as a PMB ether to afford 9. Sharpless asymmetric dihydroxylation reaction (AD-mix-α) 35 of 9 ... l) (D)-DIPT/Ti(O i Pr) 4 (1.2:1.0), t-BuOOH, MS 4 Å, CH 2 Cl 2 , −20 °C (73%); (m) (PhS) 2 , Bu 3 ...