The Journal of Organic Chemistry

1, 1-Diphenylsila-2-cyclohexanone1

AG Brook, JB Pierce

Index: Brook,A.G.; Pierce,J.B. Journal of Organic Chemistry, 1965 , vol. 30, p. 2566 - 2571

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Citation Number: 24

Abstract

(8) in about 50% yield. Diphenylsilacyclohexene, a colorless oil, shows carbon-carbon double-bond stretching absorption at 6.29 p close to the value of 6.25 p found for dichlorosila~ yclopentene.~ The nmr spectrum is complex. In the neat liquid two complex aromatic bands centered at about 6= 7.55 and 7.16 ppm are ascribable to the four ortho and six ineta plus para hydrogens, these bands coalescing in dilute solution to a single ...