Selenium-linking strategy for traceless solid-phase synthesis of acrylamides
SR Sheng, XC Wang, XL Liu, CS Song
Index: Sheng, Shou-Ri; Wang, Xing-Cong; Liu, Xiao-Ling; Song, Cai-Sheng Synthetic Communications, 2003 , vol. 33, # 16 p. 2867 - 2872
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Abstract
View all references with β-bromopropionic acid. The minimum loading of COOH of resin 3 verified by their FT-IR spectra exhibiting a strong carbonyl absorption at 1708ácm −1 was determined by acid-base titration[7]18. Schuerch , C. and Frechet , JM 1971. J. Am. Chem. Soc., 93: 492 [CrossRef] View all references to be 1.23ámmol COOH/g. Resin 3 can be stored at room temperature for long time without diminution of capacity or the liberation of disagreeable odors.
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