Biphasic sonochemistry. Convenient generation of dichlorocarbene
SL Regen, A Singh
Index: Regen, Steven L.; Singh, Alok Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1587 - 1588
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Citation Number: 65
Abstract
after 1.5 h. Similar isolated yields of dichlorocyclopropanes have been obtained for a variety of substituted alkenes and are presented in Table I. In general, reaction times and yields compare favorably with analogous phase-transfer procedures reported in the literat~ e.~" While small-scale preparations gave excellent and reproducible results, larger reactions (> 5 mmol of alkene) gave poor conversions; we assume that this is due to the limited power of ...
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