α-(N-Alkylamino)-nitriles

LJ Exner, LS Luskin…

Index: Exner et al. Journal of the American Chemical Society, 1953 , vol. 75, p. 4841

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Citation Number: 14

Abstract

4842 NOTES VOl. 75 tion was 380 g.(12.3 moles). The solution was refrigerated overnight. Distillation at reduced pressure through a column 45 cm. long packed with Berl saddles gave 675 g.(81%) of a colorless liquid, collected at 66-68'(50 mm.). The foreruns were refluxed under a water separator with 200 ml. of benzene to give 159 ml. of water. By distillation, an additional 96 g.(11.5%) of product was obtained. a-Allylaminoacetonitrile.- ...