Preparation of Triethylacetonitrile and Triethylacetic Acid

C Schuerch Jr, EH Huntress

Index: Schuerch; Huntress Journal of the American Chemical Society, 1948 , vol. 70, p. 2825

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Citation Number: 6

Abstract

4, 4'-Diketodicyclohexyl (III).-Crude 4, 4'dihydroxydicyclohexyl (11), prepared from p, p'- diphenol (I) by high pressure hydrogenation over Raney nickel catalyst by the method of Adkins, a was converted to (111) as follows. A mixture of 50 g. of (11), 50 ml. of diphenyl ether, and 13 g. of copper chromite catalyst was heated for three hours at 260-270”. During this time 70y0 of the theoretical quantity of hydrogen necessary for complete conversion to ...