The Journal of Organic Chemistry

Synthesis of dioxocarboxylic acids

RO Pendarvis, KG Hampton

Index: Pendarvis,R.O.; Hampton,K.G. Journal of Organic Chemistry, 1974 , vol. 39, p. 2289 - 2291

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Citation Number: 12

Abstract

Synthesis of Dioxocarboxylic Acids J. Org. Chem., Vol. 39, No. 15, 1974 2289 ture was stirred at room temperature for 2 hr under nitrogen. The product was filtered under nitrogen, washed (D201, and dried (P206). I t had the same melting point as that of diprotio starting material. The nmr spectrum (DMSO-&) showed the absence of NH protons in the 9.5-10.5 ppm region. Kinetics of the Reaction. An approximately 0.1 M solution of the sodium salt of ...