The Journal of Organic Chemistry

Carbanion halogenations with carbon tetrahalides.. alpha.-Halo esters

RT Arnold, ST Kulenovic

Index: Arnold,R.T.; Kulenovic,S.T. Journal of Organic Chemistry, 1978 , vol. 43, p. 3687 - 3689

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Citation Number: 57

Abstract

Analysis of Products. A mixture of aliphatic acid (10 mmol), bromine (10 mmol), chlorosulfonic acid (0.5 mL), and 1, 2-dichloroethane (50 mL) was heated at 85" C for 2 h. After unreacted bromine and 20 mL of 1, 2-dichloroethane were distilled off, methanol (30 ...