A convenient synthesis of 7-halo-1-indanones and 8-halo-1-tetralones

P Nguyen, E Corpuz, TM Heidelbaugh…

Index: Journal of Organic Chemistry, , vol. 68, # 26 p. 10195 - 10198

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Citation Number: 32

Abstract

... The Journal of Organic ... followed by addition of 2 M NaOH until the mixture was at pH 8. The aqueous layer was extracted with EtOAc and the organic fractions were ... to give 7-aminoindan- 1-one (15) as a yellow solid, 9.95 g (91%): 1 H NMR (300 MHz, CDCl 3 ) δ 7.27 (t, J = 7.2 Hz ...